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排序方式: 共有1210条查询结果,搜索用时 278 毫秒
31.
Sonia Meco Supriyo Ganguly Stewart Williams Norman McPherson 《Journal of Materials Engineering and Performance》2014,23(9):3361-3370
Fusion welding of steel to aluminum is difficult due to formation of different types of Fe-Al intermetallics (IMs). In this work, 2 mm-thick steel was joined to 6 mm aluminum in overlap configuration using a 8 kW CW fiber laser. A defocused laser beam was used to control the energy input and allow melting of the aluminum alone and form the bond by wetting of the steel substrate. Experimentally, the process energy was varied by changing the power density (PD) and interaction time separately to understand the influence of each of these parameters on the IM formation. It was observed that the IM formation is a complex function of PD and interaction time. It was also found that the mechanical strength of such joint could not be simply correlated to the IM layer thickness but also depends on the area of wetting of the steel substrate by molten aluminum. In order to form a viable joint, PD needs to be over a threshold value where although IM growth will increase, the strength will be better due to increased wetting. Any increase in interaction time, with PD over the threshold, will have negative effect on the bond strength. 相似文献
32.
Study of the effect of vintage,maturity degree,and irrigation on the amino acid and biogenic amine content of a white wine from the Verdejo variety 下载免费PDF全文
33.
Anthocyanin profile of red fruits and black carrot juices,purees and concentrates by HPLC‐DAD‐ESI/MS‐QTOF 下载免费PDF全文
Patricia Garcia‐Herrera Maria‐Luisa Pérez‐Rodríguez Teresa Aguilera‐Delgado Maria‐Jose Labari‐Reyes Begoña Olmedilla‐Alonso Montana Camara Sonia de Pascual‐Teresa 《International Journal of Food Science & Technology》2016,51(10):2290-2300
A fast and reliable method for anthocyanin extraction and identification by HPLC‐DAD‐ESI/MS‐QTOF was used to analyse the anthocyanin composition of commercial red fruit juices (blackberry, redcurrant and pomegranate), purees (strawberry, cherry and raspberry) and concentrates (elderberry, blueberry and red grape). The anthocyanin profile of black carrot juice is also reported. The extraction and analysis method allowed us to detect and quantify a wide range of individual anthocyanins in a simple and rapid way. Pelargonidin‐3‐glucoside was detected in redcurrant for the first time and petunidin‐3‐galactoside quantified for the first time in blueberries. Considering the health benefits that have been associated with anthocyanin consumption, all these fruit and vegetables processed products could appear as a good source of this group of phytochemical compounds for their direct consumption or their use as ingredients for the design of new food product or food supplements. 相似文献
34.
Susanna Esposito Alessia Scala Sonia Bianchini Alberto Zampiero Emilio Fossali Nicola Principi 《International journal of molecular sciences》2016,17(3)
In order to compare the last version of the Respiratory Virus Panel (RVP) Fast assay for human Adenovirus (hAdv) detection with a specific real-time polymerase chain reaction (qPCR), which is considered the gold standard for hAdv detection, nasopharyngeal samples collected from 309 children (age range, four months to eight years) with respiratory tract infection were tested using the RVP Fast v2 assay (Luminex Molecular Diagnostics, Inc., Toronto, ON, Canada) and a specific TaqMan qPCR to identify hAdv DNA. The RVP Fast v2 assay detected 30/61 (49.2%) hAdv infections that had been identified by real-time qPCR, demonstrating a significantly lower detection rate (p < 0.001). The sensitivity of the RVP Fast v2 assay in comparison to qPCR was lower in younger children (42.9% vs. 57.7%; Cohen’s kappa coefficient, 0.53); in samples with co-infections (40.0% vs. 56.7%; Cohen’s kappa coefficient, 0.52); and in samples with hAdv type C (45.9% vs. 57.1%; Cohen’s kappa coefficient, 0.60). Samples with lower viral loads were associated with a significantly lower sensitivity of the RVP Fast v2 assay (35.1% vs. 68.2%, p = 0.01; Cohen’s kappa coefficients, 0.49). The RVP Fast v2 assay has important limitations for the detection of hAdv and cannot be used to evaluate whether hAdvs are the main etiologic agent responsible for an outbreak or when epidemiological studies are performed. 相似文献
35.
36.
Sonia R. Merritt Agata A. Exner Zhenghong Lee Horst A. von Recum 《Advanced Engineering Materials》2012,14(5):B266-B278
Polymer processing via electrospinning is a cost effective and scalable method for preparing nanofibers with industrial, electrical, and biomedical applications, particularly tissue engineering and drug delivery. Characterization methods for these fibers include microscopy techniques for vitro surface morphology information, spectroscopy methods to determine in vitro chemical composition, and medical imaging tools for in vivo assessment of morphology and efficacy of implanted material. The focus of this paper is be on recent applications for electrospun nanofibers, in vitro characterization methods, and medical imaging modalities that can be used for in vivo assessment of the fibers, as well as insights in how to adapt existing techniques toward the characterization of electrospun materials. 相似文献
37.
Daiana Garcia Germán Barros Sofía Chulze Antonio J. Ramos Vicente Sanchis Sonia Marín 《Journal of the science of food and agriculture》2012,92(15):2952-2959
BACKGROUND: Fusarium graminearum and F. verticillioides are two very important mycotoxigenic species as they cause diverse diseases in crops. The effects of constant and cycling temperatures on growth and mycotoxin production of these species were studied on soybean based medium and on irradiated soya beans. RESULTS: F. graminearum grew better when was incubated at 15, 20 and 15–20 °C (isothermal or cycling temperature) during 21 days of incubation. Maximum levels of zearalenone and deoxynivalenol (39.25 and 1040.4 µg g?1, respectively) were detected on soya beans after 15 days of incubation and the optimal temperature for mycotoxin production was 15 °C for zearalenone and 20 °C for deoxynivalenol. F. verticillioides grew better at 25 °C in culture medium and at 15/20 °C and 15/25 °C on soybean seeds. Fumonisin B1 was produced only in culture medium, and the maximum level (7.38 µg g?1) was found at 15 °C after 7 days of incubation. CONCLUSION: When growth and mycotoxin production under cycling temperatures were predicted from the results under constant conditions, observed values were different from calculated for both species and substrate medium. Therefore, care should be taken if data at constant temperature conditions are to be extrapolated to real field conditions. Copyright © 2012 Society of Chemical Industry 相似文献
38.
Amine-terminated aromatic and semi-aromatic hyperbranched polyamides: synthesis and characterization
Saima Shabbir Sonia Zulfiqar Muhammad Ilyas Sarwar 《Journal of Polymer Research》2011,18(6):1919-1929
A facile synthetic approach to aromatic and semiaromatic amine-terminated hyperbranched polyamides via direct polymerization
of triamine (B3) with different diacid chlorides (A2) was explored. An aromatic triamine, 1,3,5-tris(4′-aminophenylcarbamoyl)benzene (TAPCB), was synthesized and monomers were characterized by elemental analysis, FTIR, 1H and 13C NMR spectroscopy. Finally, the polycondensation reaction of TAPCB with terephthaloyl chloride (TPC), isophthaloyl chloride
(IPC), sebacoyl chloride (SC) and adipoyl chloride (AC) resulted in the preparation of four hyperbranched polyamides i.e.,
HBPA 1, 2, 3 and 4, respectively. FTIR and 1H NMR analyses confirmed the structures of the ensuing polymers and DB was found between 0.51–0.55. These thermally stable
amorphous HBPAs were soluble in polar aprotic solvents at room temperature having glass transition temperatures (Tg) between 138–198 °C. Inherent viscosities (ηinh) and weight average molecular weights (Mw) were in the range of 0.27–0.35 dL/g and 1.3 × 104–2.7 × 104, respectively. Future prospects are envisaged. 相似文献
39.
Sonia Ahangar Ghader Rezazadeh Rasool Shabani Goodarz Ahmadi Alireza Toloei 《International Journal of Mechanics and Materials in Design》2011,7(4):327-342
In this paper, the size-dependent vibrational behavior of a microbeam conveying fluid was investigated using the Modified
Couple Stress Theory. For cantilever and clamped-clamped microbeams, the small amplitude vibration equation of the micro-beams
was solved using a Galerkin based reduced order model and the effects of material length-scale parameter on its natural frequencies
were evaluated. It was found that for the both cantilever and clamped-clamped conditions, the critical fluid velocities predicted
by the modified couple stress theory are higher than those predicted by the classical beam theory. In addition, the differences
between the eigen-frequencies and the critical fluid velocities predicted by the modified couple stress theory and classical
beam theory depends on the ratio of the material length-scale parameter to the beam height. In addition an unexpected result
in the difference between the first eigen-frequency of the cantilever micro-beam obtained by the classical and the modified
couple stress theory has been achieved. 相似文献
40.
Synergistic effect of organoclay fillers based on fluorinated surfmers for preparation of polystyrene nanocomposites 下载免费PDF全文
Chahinez Benbayer Salima Saidi‐Besbes Elisabeth Taffin de Givenchy Sonia Amigoni Frédéric Guittard Aicha Derdour 《应用聚合物科学杂志》2015,132(33)
Novel fluorinated reactive surfactants were used for the organic modification of monmorillonite clays. These organoclays were used for the preparation of polystyrene?clay nanocomposites by in‐situ free radical polymerization. Reference systems based on hydrocarbon homologous surfmer and nonpolymerizable surfactants were also used to deduce the effect of the fluorine moiety and the polymerizable function on the morphology and thermal stability of the prepared nanocomposites. Different structural parameters of the surfactants were investigated and modulated for the clay modification including: the nature of surfactant (surfmer/classical surfactant, fluorinated, or hydrocarbonated), the length of the fluorinated chain as well as the length of the hydrocarbon spacers linking the ammonium head to the fluorine chain or the polymerizable acrylic function. Wide angle‐X‐ray scattering (WAXD), thermogravimetric analysis (TGA), and electronic microcopies (TEM and SEM) were used to establish a structure‐morphology, thermal properties relationships, and to highlight the key parameters governing the exfoliation process. © 2015 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2015 , 132, 42347. 相似文献